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1 N-Alkylation of NH-1,2,3-Triazoles with Alkylhalides . . . . . . . . . . . . . . . . 2 Alkylation of NH-1,2,3-Triazoles with Alkyl Carboxylates and Sulf(on)ates . . . . N. Belskaya (*), J. Subbotina, and S. Lesogorova Ural Federal University, Mira Str. ru 53 56 56 58 59 60 61 64 65 66 68 70 77 78 82 52 N. Belskaya et al. 3 Mitsunobu Reaction of NH-1,2,3-Triazoles . . . . . . . . . . . . . . . . . . . . . 4 Michael Addition . . . . . . . . . .

CaCl 2 , 75 °C, 30 min 209 Ar 2 Ar OH 2. Rh 2(S-PTAD) 4, CHCl 3, rt, 1-36 h 1 H N SO2 R1 211 major Ar 2 Ar1 H N SO2 R1 212 minor Ar2 B OH 210 R 1 = Me, i-Pr, 4-Me-C 6 H4 , 4-Cl-C 6 H4 , 4-MeO-C 6H 4 , 4-CF3 -C 6 H4 ; Ar1 = Ph, 4-Me-C 6 H4 , 4-CF 3-C6 H4 , 3-CF3 -C 6 H4 ; Ar2 = naphth-1-yl, 3-CF3 -C 6H 4, 4-MeO-C 6H 4, MeC(O)-C 6H 4, 3-Br-C 6 H4 , 3-NO 2-C6 H4 , 4-F-C 6 H4 , 4-F-C 6 H4 Scheme 63 Synthesis of N-sulfonyl enamines 211 and 212 donor/acceptor carbenes in which the donor group is a protected amine functionality (see Sect.

4 Intramolecular Cyclization of Bis(hydrazones) and Hydrazonoamidoximes . . . . 5 Boulton–Katritzky Rearrangement of 3-Hydrazono Oxadiazoles, -Furoxans and -Isoxazoles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 Intra- and Intermolecular Reactions of Diazocompounds . . . . . . . . . . . . . . . . . 7 Heterocycle Transformations in the Synthesis of 2H-1,2,3-Triazoles . . . . . . . . . .

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